HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 59198432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 14994648 | HCID 14994648 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59198432 | HCID 59198432 | — |
Reaction Steps
To a suspension of [1]benzothieno[3,2-c]pyridin-1(2H)-one in AcOH (0.52 M) was added Br2 (1.1 equiv) at room temperature. The mixture was heated to reflux for 1.5 h, cooled to room temperature, poured into H2O and stirred for 30 min. The mixture was filtered and washed with H2O to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518964B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-10872ab922b04fd9a83f2a93239c434c |
| Source note | uspto-grants-2013_08 |