Phosphorus oxychloride → HCID 86639256, compound

Participants

Reaction Steps

A solution of the product from Step 1 in POCl3 (0.057 M) was set up on the Smith Creator microwave reactor for 10 min at 175° C. The resulting solution was poured onto cold saturated NaHCO3 solution and the suspension was stirred until all the reagent was consumed and the final pH was 7-8. The suspension was then filtered to give the title compound as an off-white solid.

Provenance & Evidence