HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-(4-Fluorophenyl)-2-oxoethyl thiocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Bromo-1-(4-fluorophenyl)ethan-1-one | HCID 96749 | — |
| Reactant | Sodium thiocyanate | HCID 516871 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(4-Fluorophenyl)-2-oxoethyl thiocyanate | HCID 4198992 | — |
Reaction Steps
10 g (46 mmol) of 2-bromo-1-(4-fluorophenyl)ethanone and 3.74 g (46 mmol) of sodium thiocyanate were stirred in 80 ml ethanol at 50° C. for 2 h. After addition of water the separated solid was isolated by filtration, washed and dried. Yield: 8.96 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518976B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-cac41fc3dcc144c4a528f96636b9ede9 |
| Source note | uspto-grants-2013_08 |