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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1896950Generated: October 31, 2026

HCID 58562734, compound → HCID 68003608, compound

https://huagongshe.com/reaction/1896950

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58562734HCID 58562734—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 68003608HCID 68003608—

Reaction Steps

Into a 50-mL round-bottom flask, was placed a solution of tert-butyl 3-(2-(6-(trifluoromethyl)cinnolin-4-ylamino)acetamido)azetidine-1-carboxylate (140 mg, 0.33 mmol,) in dichloromethane (10 ml) and CF3COOH (1 ml). The reaction mixture was stirred for 2 h at room temperature. The resulting mixture was concentrated under vacuum to give the title compound as yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08518969B2
Source datasetuspto-grants-2013_08
ORD IDord-469f080e3c014713803c74177ceaea01
Source noteuspto-grants-2013_08