HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58562734, compound → HCID 68003608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58562734 | HCID 58562734 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68003608 | HCID 68003608 | — |
Reaction Steps
Into a 50-mL round-bottom flask, was placed a solution of tert-butyl 3-(2-(6-(trifluoromethyl)cinnolin-4-ylamino)acetamido)azetidine-1-carboxylate (140 mg, 0.33 mmol,) in dichloromethane (10 ml) and CF3COOH (1 ml). The reaction mixture was stirred for 2 h at room temperature. The resulting mixture was concentrated under vacuum to give the title compound as yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518969B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-469f080e3c014713803c74177ceaea01 |
| Source note | uspto-grants-2013_08 |