HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 4-Phenoxy-2,5-dimethylnitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Chloro-2,5-dimethyl-4-nitrobenzene | HCID 252793 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-Phenoxy-2,5-dimethylnitrobenzene | HCID 68594119 | — |
Reaction Steps
A solution of 4.44 g (47 mmol) of phenol and 8.76 g (47 mmol) of 2,5-dimethyl-4-chloro-nitrobenzene in 50 ml of DMF was admixed with 9.78 g (71 mmol) of K2CO3 and the mixture was heated under reflux for 10 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519003B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-e30873f34018492d8853a23790373604 |
| Source note | uspto-grants-2013_08 |