Hydrochloric Acid → HCID 86594427, compound

HRID 1897498Notes

Reaction equation

HRID 1897498 reaction equation
[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH:13]C(OC(C)(C)C)=O)[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8].[ClH:22]>>[ClH:22].[ClH:22].[CH3:1][O:2][C:3](=[O:21])[C@@H:4]([NH2:13])[CH2:5][CH2:6][N:7]([CH2:9][CH2:10][O:11][CH3:12])[CH3:8]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86594426HCID 86594426, compound

Product 1

HCID 86594427HCID 86594427, compound

Procedure

(S)-2-tert-Butoxycarbonylamino-4-[(2-methoxyethyl)-methylamino]-butyric acid methyl ester (0.086 g, 0.28 mmol) was treated with HCl (1 mL of 4M in dioxane) and sonicated. The mixture was concentrated and dried under high vacuum to provide the product.

Workup

  1. customsonicated
  2. concentrationThe mixture was concentrated
  3. customdried under high vacuum
  4. customto provide the product

Sources & evidence

ORD record
ord-c61b1ba44a41445485bcc6c9346e342e
Source dataset
uspto-grants-2013_08
Patent number
US08518983B2

Reaction notes

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