HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 6-Fluoro-2-naphthoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-Fluoro-2-naphthoic acid | HCID 2782788 | — |
| Product | 6-Fluoro-2-naphthoyl chloride | HCID 86674834 | — |
Reaction Steps
6-fluoro-2-naphthoic acid (2 g, 10.52 mmol) was stirred in thionyl chloride (21.03 ml) at 80° C. for 4 h in pressure vessel. The mixture was cooled and concentrated. The acid chloride was dried and used as is for next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519134B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-9bce67345cf24d389ebf4192955b9154 |
| Source note | uspto-grants-2013_08 |