Chlorosuccinimide → 4-Chloro-3-isopropylaniline

HRID 1898234Notes

Reaction equation

[CH:1]([C:4]1[CH:5]=[C:6]([NH2:10])[CH:7]=[CH:8][CH:9]=1)([CH3:3])[CH3:2].C1C(=O)N([Cl:18])C(=O)C1>>[Cl:18][C:9]1[CH:8]=[CH:7][C:6]([NH2:10])=[CH:5][C:4]=1[CH:1]([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 31398Chlorosuccinimide

HCID 4586793-Isopropylaniline

Product 1

HCID 198914954-Chloro-3-isopropylaniline

Procedure

Prepared from 7.84 g of 3-iso-propyl-phenylamine and 7.75 g NCS. Yield: 4.6 g. LC-MSD, m/z for C9H12ClN [M+H]+=170.2, 172.0;

Sources & evidence

ORD record: ord-5befb423c301415fb172648ec0fc4a5f
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08519135B2

Reaction notes

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