3-Ethylaniline → 93-49-2

HRID 1898235Notes

Reaction equation

[CH2:1]([C:3]1[CH:4]=[C:5]([NH2:9])[CH:6]=[CH:7][CH:8]=1)[CH3:2].C1C(=O)N([Cl:17])C(=O)C1>>[Cl:17][C:8]1[CH:7]=[CH:6][C:5]([NH2:9])=[CH:4][C:3]=1[CH2:1][CH3:2]

Participants

Reactant 2

HCID 114753-Ethylaniline

HCID 31398Chlorosuccinimide

Product 1

HCID 2071434793-49-2

Procedure

Prepared from 7.36 g of 3-ethyl-phenylamine and 8.12 g NCS. Yield: 4.4 g. LC-MSD, m/z for C8H10ClN [M+H]+=156.0, 158.0;

Sources & evidence

ORD record: ord-5f133dc978d84020822d334a72e11166
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08519135B2

Reaction notes

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