HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-2-bromo-5-chloropyridine → HCID 58268262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-2-bromo-5-chloropyridine | HCID 2769640 | — |
| Reactant | HCID 58268035 | HCID 58268035 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 58268262 | HCID 58268262 | — |
Reaction Steps
Prepared from 1.71 g (7.15 mmol) of 4-chloro-3-ethyl-benzenesulfonyl chloride and 1.34 g (6.47 mmol) of 2-bromo-5-chloro-pyridin-3-ylamine in 4 mL pyridine using procedure x. Yield: 2.35 g of a white solid. LC-MSD, m/z for C13H11BrCl2N2O2S [M+H]+=408.8, 410.8, 412.8
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519135B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-dfb5bd4a7c6044c2acb17613ee222365 |
| Source note | uspto-grants-2013_08 |