HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-2-bromo-5-chloropyridine → HCID 58268301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-2-bromo-5-chloropyridine | HCID 2769640 | — |
| Reactant | HCID 58268146 | HCID 58268146 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 58268301 | HCID 58268301 | — |
Reaction Steps
Prepared from 420 mg (1.57 mmol) of 3-tert-butyl-4-chloro-benzenesulfonyl chloride and 326 mg (1.57 mmol) of 2-bromo-5-chloro-pyridin-3-ylamine in 3 mL pyridine using procedure x. Yield: 0.48 g of a white solid. LC-MSD, m/z for C15H15BrCl2N2O2S [M+H]+=436.9, 438.8, 440.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519135B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-2a5b55a4326145f78e73f42360fd4a4a |
| Source note | uspto-grants-2013_08 |