HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-2-bromo-5-chloropyridine → HCID 58268062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-2-bromo-5-chloropyridine | HCID 2769640 | — |
| Reactant | 3-Acetyl-4-chlorobenzene-1-sulfonyl chloride | HCID 43118905 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 58268062 | HCID 58268062 | — |
Reaction Steps
Prepared from 1.6 g (6.32 mmol) of 3-acetyl-4-chloro-benzenesulfonyl chloride and 1.3 g (6.28 mmol) of 2-bromo-5-chloro-pyridin-3-ylamine in 8 mL pyridine using procedure x. Yield: 1.3 g of a white solid. LC-MSD, m/z for C13H9BrCl2N2O3S [M+H]+=422.8, 424.8, 426.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519135B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-a6fa1b10617f43ae91cd3e6a96f238a7 |
| Source note | uspto-grants-2013_08 |