HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-2-bromo-5-chloropyridine → HCID 58268115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-2-bromo-5-chloropyridine | HCID 2769640 | — |
| Reactant | HCID 58268227 | HCID 58268227 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 58268115 | HCID 58268115 | — |
Reaction Steps
Prepared from 377 mg (1.37 mmol) of 4-chloro-3-(1,1-difluoro-ethyl)-benzenesulfonyl chloride and 270 mg (1.30 mmol) of 2-bromo-5-chloro-pyridin-3-ylamine in 2 mL pyridine using procedure x. Yield: 460 mg of a white solid. LC-MSD, m/z for C13H9BrCl2F2N2O2S [M+H]+=444.8, 446.8, 448.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519135B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-456cd2a6940a48229ecc4a446e5f18ed |
| Source note | uspto-grants-2013_08 |