Chloromethyl Methyl Ether → HCID 58268037, compound

Participants

Reaction Steps

Prepared from 2.35 g (5.73 mmol) of N-(2-bromo-5-chloro-pyridin-3-yl)-4-chloro-3-ethyl-benzenesulfonamide, 2.76 g of potassium carbonate and 1.3 mL of methoxymethyl chloride in 10 mL THF using procedure x. Yield: 980 mg of a white solid. LC-MSD, m/z for C15H15BrCl2N2O3S [M+H]+=452.9, 454.9, 456.9

Provenance & Evidence