反应详情

A mixture of 7-chloro-3H-imidazo[4,5-b]pyridine (1.47 g, 9.64 mmol) and 15 mL of 57% hydriodic acid were reacted at 80° C. for 4 h. After the solid was filtered off it was resubmitted to the reaction with 10 mL of fresh 57% hydriodic acid. The reaction yielded 1.3 g of the product as a black powder, 90% pure.

1. customwere reacted at 80° C. for 4 h
2. filtrationAfter the solid was filtered off it
3. customwas resubmitted to the reaction with 10 mL of fresh 57% hydriodic acid