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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1898305Generated: November 2, 2026

Thiophosgene → HCID 18464324, compound

https://huagongshe.com/reaction/1898305

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThiophosgeneHCID 10040—
Reactant2-tert-ButylanilineHCID 80574—
ReactantDiisopropylethylamineHCID 81531—
ProductHCID 18464324HCID 1846432447.5%

Reaction Steps

The title compound was prepared following the procedure described for intermediate-2 using 2-tert-butylaniline (5.0 g, 0.033 mol), thiophosgene (3.80 g, 0.033 mol) and N-ethyl di-isopropyl amine (8.5 g, 0.066 mol) to afford 3.0 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08519149B2
Source datasetuspto-grants-2013_08
ORD IDord-4e1a172fb4e242a6abb58dae9e18c706
Source noteuspto-grants-2013_08