HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 178507581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 2-Amino-5-(trifluoromethyl)pyridine | HCID 735862 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178507581 | HCID 178507581 | — |
Reaction Steps
The title compound was prepared by following the procedure described for Intermediate-40 using 5-(trifluoromethyl)pyridin-2-amine (0.500 g, 3.08 mmol), acetic acid (5.0 mL) and 50% hydrogen peroxide (2.0 mL) to afford 0.475 g of the desired product. 1HNMR (DMSO-d6): δ 6.88 (d, J=8.7 Hz, 1H), 7.40 (d, J=8.7 Hz, 1H), 7.49 (s, 2H), 8.49 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519149B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-0f7cf4e279b94ff2be69d32fe60b0f99 |
| Source note | uspto-grants-2013_08 |