HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178422741, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178422740 | HCID 178422740 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178422741 | HCID 178422741 | 112.5% |
Reaction Steps
The title compound was prepared following the procedure described for Example-146 using N-(4-bromophenyl)-2-[(2,6-dichlorophenyl)amino]-7,7-dimethyl-7,8-dihydro-1H-furo[3,2-e]benzimidazole-5-carboxamide (Example-11, 0.100 g), THF and conc. HCl to afford 0.060 g of the desired product. 1HNMR (DMSO-d6): δ 1.56 (s, 6H), 2.20 (s, 2H), 7.51-7.57 (m, 3H), 7.64-7.74 (m, 5H), 9.81 (s, 1H), 12.0-13.0 (br, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519149B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-100934a16af748e3bce8053d06a46f10 |
| Source note | uspto-grants-2013_08 |