HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 53856516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 53894677 | HCID 53894677 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53856516 | HCID 53856516 | 102.2% |
Reaction Steps
A mixture of 2-(3,4-difluorophenyl)-3-[4-(methylthio)phenyl]acrylic acid (12 g) and phosphorus pentachloride (9.0 g) in dichloromethane (120 ml) was stirred for 1 hour. The solvent was evaporated to give a solid of 2-(3,4-difluorophenyl)-3-[4-(methylthio)phenyl]acryloyl chloride (13 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05571810 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-8c811f620af845b1a74e4e191b94c9eb |
| Source note | uspto-grants-1996_11 |