HRID1899694

反应详情

EQUATION

反应方程式

HRID 1899694 的结构方程式

PROCEDURE

实验过程

N-(4-Methyl-3-trifluoromethyl-5-isoxazolyl)-1-naphthalenesulfonamide was prepared, as described in Example 90, from 5-amino-4-methyl-3-trifluoromethylisoxazole and 1-naphthalenesulfonyl chloride in 85% yield. Purification was achieved by recrystallization from methanol/water to give white needed, m.p. 154°-155° C.

WORKUP

后处理

  1. customPurification
  2. customwas achieved by recrystallization from methanol/water
  3. customto give white