HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 67623101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 53927178 | HCID 53927178 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67623101 | HCID 67623101 | 61.5% |
Reaction Steps
Diastereomer A of 3-(3-morpholino-1-phenylpropyl)-5-phenyl-1,3-oxazolidin-2-one (480 mg, 1.31 mmol) prepared in the same manner as is described in Example 7 and fumaric acid (152 mg, 1.31 mmol) were dissolved in ethanol (30 ml). The resulting solution was concentrated by distillation under reduced pressure to obtain 389 mg of the titled compound as a pale yellow amorphous product (yield: 61.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05574030 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-349d4d86b2c84d1abeba56208a0ee6df |
| Source note | uspto-grants-1996_11 |