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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1899982Generated: October 30, 2026

Benzyl Bromide → HCID 18923724, compound

https://huagongshe.com/reaction/1899982

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl BromideHCID 7498—
ReactantTriethylamineHCID 8471—
Reactant3,5-Dichloro-N-methylanilineHCID 12377757—
SolventAcetonitrileHCID 6342—
ProductHCID 18923724HCID 18923724—

Reaction Steps

The mixture of 3,5-dichloro-N-methylaniline (345 mg) and excess amount of benzyl bromide and triethylamine in acetonitrile (7 ml) was refluxed for 4 hours. The reaction mixture was separated with ethyl acetate and water, and the organic layer was washed with water, dried and concentrated in vacuo to give N-benzyl-3,5-dichloro-N-methylaniline (532 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05574042
Source datasetuspto-grants-1996_11
ORD IDord-452cdeaf38954dea8814a7e87e8f77f0
Source noteuspto-grants-1996_11