反应详情

The mixture of 3,5-dichloro-N-methylaniline (345 mg) and excess amount of benzyl bromide and triethylamine in acetonitrile (7 ml) was refluxed for 4 hours. The reaction mixture was separated with ethyl acetate and water, and the organic layer was washed with water, dried and concentrated in vacuo to give N-benzyl-3,5-dichloro-N-methylaniline (532 mg).

1. temperaturewas refluxed for 4 hours
2. customThe reaction mixture was separated with ethyl acetate and water
3. washthe organic layer was washed with water
4. customdried
5. concentrationconcentrated in vacuo