HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67626277, compound → HCID 67626423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67626277 | HCID 67626277 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67626423 | HCID 67626423 | 298.7% |
Reaction Steps
3-Bromo-8-[3-[N-(tert-butoxycarbonyl-L-prolylglycyl)-N-methylamino]-2,6-dichlorobenzyloxy]-2-methylimidazo[1,2-a]pyridine (67 mg) was dissolved in 4N solution of hydrogen chloride in ethyl acetate (3 ml). The solution was evaporated in vacuo to give 3-bromo-8-[2,6-dichloro-3-[N-(L-prolylglycyl)-N-methylamino]benzyloxy]-2-methylimidazo[1,2-a]pyridine dihydrochloride (64 mg) as colorless glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05574042 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-fce166de6f4f46708ea43c7958c24e76 |
| Source note | uspto-grants-1996_11 |