HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 88282627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzyltriethylammonium | HCID 17208 | — |
| Reactant | HCID 86749985 | HCID 86749985 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 88282627 | HCID 88282627 | — |
Reaction Steps
1.8 g (10 mmoles) of 2-hydroxyiminomethyl-phenylacetic acid are reacted with 1.50 ml of iodomethane, 5 g of potassium carbonate and 10 mg of triethylbenzylammonium (TEBA) chloride in 20 ml of anhydrous acetonitrile. The system is left for 6 hours at +80° C. and overnight at ambient temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05574153 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-c735d32531ef4eea82c7e2c516d65b43 |
| Source note | uspto-grants-1996_11 |