HuagongsheHuagongshe Chemistry Print Report · For research reference only
(-)-(2R,5S)-1-allyl-2,5-dimethylpiperazine → HCID 23372082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (-)-(2R,5S)-1-allyl-2,5-dimethylpiperazine | HCID 10534891 | — |
| Reactant | HCID 21480428 | HCID 21480428 | — |
| Reactant | HCID 178418385 | HCID 178418385 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23372082 | HCID 23372082 | — |
Reaction Steps
Crude 3-((2R,5S)-4-allyl-2,5-dimethyl-1-piperazinyl)-3-(1H-benzotriazol-1-yl)methyl)-N-(3-fluorophenyl)-N-methylbenzamide was prepared from (2R,5S)-1-allyl-2,5-dimethylpiperazine (1.89 g), benzotriazole (1.39 g), and N-(3-fluorophenyl)-3-formyl-N-methylbenzamide (3.0 g) in toluene as described in Example 16. Method B.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05574159 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-d786da050ed54eb88a5c05972dad329f |
| Source note | uspto-grants-1996_11 |