HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 23369740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23369609 | HCID 23369609 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23369740 | HCID 23369740 | 57.5% |
Reaction Steps
The title compound was prepared in a manner similar to that described in Example 274 using the compound obtained in Example 292 (46 mg, 0.14 mmol), sodium azide (53 mg, 0.82 mmol) and dimethylformamide (1.0 ml). 24 mg of the title compound was obtained as a pale yellow solid (58.8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-6efdf1e7ad9e49ce8bf07c350259088d |
| Source note | uspto-grants-1996_11 |