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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1900831Generated: November 1, 2026

Allyl iodide → HCID 131719644, compound

https://huagongshe.com/reaction/1900831

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl iodideHCID 11166—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 137226530HCID 137226530—
SolventChloroform hexaneHCID 21585165—
ProductHCID 131719644HCID 13171964492.6%

Reaction Steps

Using 5-hydroxy-3,3,8-trimethylcarbostyril (2.0 g, 9.77 mmol), allyl iodide (1.72 g, 10.2 mmol), and potassium carbonate (3 g, 21.7 mmol), the procedure of Reference Example 41 was followed (reaction, post-treatment, and recrystallization from chloroform-n-hexane). 2.2 g of the title compound was obtained as colorless flakes (92.0%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05576324
Source datasetuspto-grants-1996_11
ORD IDord-2dc742880ae140aab74c7060e22315f5
Source noteuspto-grants-1996_11