HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl iodide → HCID 131719644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl iodide | HCID 11166 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 137226530 | HCID 137226530 | — |
| Solvent | Chloroform hexane | HCID 21585165 | — |
| Product | HCID 131719644 | HCID 131719644 | 92.6% |
Reaction Steps
Using 5-hydroxy-3,3,8-trimethylcarbostyril (2.0 g, 9.77 mmol), allyl iodide (1.72 g, 10.2 mmol), and potassium carbonate (3 g, 21.7 mmol), the procedure of Reference Example 41 was followed (reaction, post-treatment, and recrystallization from chloroform-n-hexane). 2.2 g of the title compound was obtained as colorless flakes (92.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-2dc742880ae140aab74c7060e22315f5 |
| Source note | uspto-grants-1996_11 |