HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 23369774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23369804 | HCID 23369804 | — |
| Product | HCID 23369774 | HCID 23369774 | 86.1% |
Reaction Steps
Using the compound obtained in Example 299 (1.93 g 5.96 mmol) and sodium azide (2.8 g, 43.1 mmol), the procedure of Example 278 was followed (reaction, post-treatment, and recrystallization from chloroform-ether). 1.47 g of the title compound was obtained as colorless crystals (86.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-b5c13d7af6fe4201ac399e1830df0a3c |
| Source note | uspto-grants-1996_11 |