n-Heptyl isocyanate → HCID 23370093, compound

Participants

Reaction Steps

To a solution of N-(4-dimethylaminophenyl)-2-aminobenzamide (1.5 g) in dichloromethane (20 ml), heptyl isocyanate (2.4 g) was added under ice-cooling and the mixture was stirred overnight while returning slowly to room temperature. The solvent was distilled off and crystallization of the residue from chloroform/ethyl acetate afforded N-(4-dimethylaminophenyl)-2-(3-heptylureido)benzamide (1.6 g, 69%).

Provenance & Evidence