HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 23370133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 23370093 | HCID 23370093 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23370133 | HCID 23370133 | 99% |
Reaction Steps
To a solution of N-(4-dimethylaminophenyl)-2-(3-heptylureido)benzamide (0.70 g) in ethanol (10 ml) was added 4N-HCl/ethyl acetate solution (0.48 ml) under ice-cooling, and the mixture was concentrated to dryness to give N-(4-dimethylaminophenyl)-2-(3-heptylureido)benzamide monohydrochloride (0.77 g, 99%) as a non-crystallizable solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576335 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-6da0f5422460465db283bbdc34e78157 |
| Source note | uspto-grants-1996_11 |