HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylamine → 1-(4-Methoxy-2-nitrophenyl)-3-cyclopentylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Reactant | phenyl N-(4-methoxy-2-nitrophenyl)carbamate | HCID 16227844 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 1-(4-Methoxy-2-nitrophenyl)-3-cyclopentylurea | HCID 23370090 | 91% |
Reaction Steps
Phenyl 4-methoxy-2-nitrophenylcarbamate (1.1 g) and cyclopentylamine (0.37 g) were dissolved in xylene (10 ml) and the solution was heated under reflux for 2 hrs. After allowing the reaction solution to cool, the crystals formed was filtered, washed with xylene, and dried to give 1-(4-methoxy-2-nitrophenyl)-3-cyclopentylurea (0.97 g, 87%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576335 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-a2c76ab4e8464bacbcbdfb48d03b9e16 |
| Source note | uspto-grants-1996_11 |