HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-iodo-, methyl ester → HCID 23370220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-iodo-, methyl ester | HCID 69132 | — |
| Reactant | 4-(Tri-n-butylstannyl)pyridine | HCID 2737318 | — |
| Reactant | 1-(Benzyloxy)-3-bromo-5-fluorobenzene | HCID 11254516 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Solvent | Phenol | HCID 996 | — |
| Product | HCID 23370220 | HCID 23370220 | — |
Reaction Steps
Following the procedures described in Phenol 1, Steps 2 and 3, but substituting O-(3,4-dimethoxy)benzyl-3-fluoro-5-trimethylstannylphenol for 4-tributylstannylpyridine and methyl 2-iodobenzoate for O-benzyl-3-bromo-5-fluorophenol, the title compound was obtained as an oil after chromatography (silica gel; hexane/EtOAc 95:5-85:15)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576338 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-db92b4f802b248d7bc88550a379b9a5a |
| Source note | uspto-grants-1996_11 |