Methyl Methacrylate → HCID 86750009, compound

HRID 1901146Notes

Reaction equation

HRID 1901146 reaction equation
[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:13][CH2:14][CH:15]1[O:17][CH2:16]1)(=[O:12])[C:9]([CH3:11])=[CH2:10].[C:18]([O:23][CH2:24][CH2:25][OH:26])(=[O:22])[C:19]([CH3:21])=[CH2:20]>>[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:13][CH2:14][CH:15]1[O:17][CH2:16]1)(=[O:12])[C:9]([CH3:11])=[CH2:10].[C:18]([O:23][CH2:24][CH2:25][OH:26])(=[O:22])[C:19]([CH3:21])=[CH2:20]

Participants

4

Reactant 3

HCID 6658Methyl MethacrylateHCID 7837Glycidyl methacrylateHCID 133602-Hydroxyethyl Methacrylate

Product 1

HCID 86750009HCID 86750009, compound

Procedure

Using methyl methacrylate (35.0 g, 0.35 mole), glycidyl methacrylate (28.4 g, 0.2 mole) and 2-hydroxyethyl methacrylate (13.0 g, 0.1 mole), the polymerization was carried out in the same manner as described in Synthesis Example 12, (1), and the precipitate was filtered and dried under reduced pressure to give 70.3 g of poly(methyl methacrylate/glycidyl methacrylate/2-hydroxyethyl methacrylate) as white powders having Mw 35000 and Mn 192000 (GPC with polystyrene calibration).

Workup

  1. customas described in Synthesis Example 12, (1),
  2. filtrationthe precipitate was filtered
  3. customdried under reduced pressure

Sources & evidence

ORD record
ord-53d9cd2df32e4768ace856e527cc5aa9
Source dataset
uspto-grants-1996_11
Patent number
US05576359

Reaction notes

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