HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tyrosol → 2-[4-(2-Oxopropoxy)phenyl]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tyrosol | HCID 10393 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromoacetone | HCID 11715 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-[4-(2-Oxopropoxy)phenyl]ethanol | HCID 21832165 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 3, but using 10 g of 2-(4-hydroxyphenyl)-ethanol, 21.6 g of bromoacetone, 30 g of potassium carbonate and 100 ml of dimethylformamide, the title compound was obtained having an Rf=0.31 (thin layer chromatography over silica gel, using a 1:1 by volume mixture of hexane and ethyl acetate as the developing solvent).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576340 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-f844bf5cf29d49ef93d3b36ff7fddb07 |
| Source note | uspto-grants-1996_11 |