Dicyclohexylcarbodiimide → S-(4-Isothiocyanatophenyl) 4-pentylthiobenzoate

HRID 1901401Notes

Reaction equation

HRID 1901401 reaction equation
[CH2:1]([C:6]1[CH:14]=[CH:13][C:9]([C:10]([OH:12])=O)=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[N:15]([C:18]1[CH:23]=[CH:22][C:21]([SH:24])=[CH:20][CH:19]=1)=[C:16]=[S:17].C1(N=C=NC2CCCCC2)CCCCC1>CN(C)C1C=CN=CC=1>[CH2:1]([C:6]1[CH:7]=[CH:8][C:9]([C:10]([S:24][C:21]2[CH:22]=[CH:23][C:18]([N:15]=[C:16]=[S:17])=[CH:19][CH:20]=2)=[O:12])=[CH:13][CH:14]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

5

Reactant 3

HCID 10868DicyclohexylcarbodiimideHCID 334794-Pentylbenzoic acidHCID 233673904-Isothiocyanatobenzene-1-thiol

Product 1

HCID 88290024S-(4-Isothiocyanatophenyl) 4-pentylthiobenzoate

Reagents, catalysts & solvents 1

HCID 142844-(Dimethylamino)pyridineCatalyst

Procedure

(18). Quantities: compound 17 (4.00 g, 0.021 mol), compound 3 (2.59 g, 0.016 mol), N,N'-dicyclohexylcarbodiimide (3.95 g, 0.019 mol), 4-(dimethylamino)pyridine (0.79 g, 0.019 mol).

Sources & evidence

ORD record
ord-7afabc2f88724637a4798af1a44f8918
Source dataset
uspto-grants-1996_11
Patent number
US05578242

Reaction notes

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