Carbon Disulfide → HCID 86750024, compound

HRID 1901403Notes

Reaction equation

HRID 1901403 reaction equation
Br[C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([S:12][CH2:13][CH2:14][CH2:15][CH3:16])[CH:8]=2)[CH:3]=1.[Mg].[C:18](=[S:20])=[S:19]>>[CH2:13]([S:12][C:7]1[CH:8]=[C:9]2[C:4](=[CH:5][CH:6]=1)[CH:3]=[C:2]([C:18]([SH:20])=[S:19])[CH:11]=[CH:10]2)[CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 3

HCID 6348Carbon DisulfideHCID 5462224MagnesiumHCID 15474603HCID 15474603, compound

Product 1

HCID 86750024HCID 86750024, compound

Procedure

Compound 12 (3.71 g, 0.013 mol), magnesium turnings (0.94 g, 0.039 mol), carbon disulphide (1.09 g, 0.014 mol). A purple solid was obtained.

Workup

  1. customA purple solid was obtained

Sources & evidence

ORD record
ord-a8f293ba40ba4fc3b6f7aa488d94a51a
Source dataset
uspto-grants-1996_11
Patent number
US05578242

Reaction notes

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