HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl 6-aminohexanoate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 6-Aminohexanoic Acid | HCID 564 | — |
| Reactant | Methanol | HCID 887 | — |
| Product | Methyl 6-aminohexanoate hydrochloride | HCID 11499324 | 99% |
Reaction Steps
Hydrogen chloride (gas) was added to a solution of 20.0 g (152 mmol) of 6-aminocaproic acid in 250 ml of methanol via rapid bubbling for 2-3 minutes. The mixture was stirred at 15°-25° C. for 3 hours and then concentrated to afford 27.5 g of the product as a white solid (99%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578287 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-61d19d3f790f4d868c962515aceaa300 |
| Source note | uspto-grants-1996_11 |