HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86750025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 6-Bromohexanoic acid | HCID 20210 | — |
| Product | HCID 86750025 | HCID 86750025 | 90% |
Reaction Steps
Hydrogen chloride (gas) was added to a solution of 5.01 g (25.7 mmol) of 6-bromocaproic acid in 250 ml of methanol via vigorous bubbling for 2-3 minutes. The mixture was stirred at 15°-25° C. for 3 hours and then concentrated to afford 4.84 g of the product as a yellow oil (90%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578287 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-eb9a9e990b7f4503a9072978612a0aba |
| Source note | uspto-grants-1996_11 |