HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23368461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 23368395 | HCID 23368395 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23368461 | HCID 23368461 | — |
Reaction Steps
To 20 ml of an ethyl acetate solution of 2 g of 3-(2-aminopentyloxy)-1,2-benzoisoxazole is added 20 ml of a dioxane solution (2.2N) of hydrogen chloride, and the crystals precipitated are collected by filtration to obtain 1.05 g of colorless, crystalline 3-(2-aminopentyloxy)-1,2-benzoisoxazole hydrochloride having a melting point of 205.8°-206.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578627 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-5c8676b4d9ff43c99c2e7ab3460facf2 |
| Source note | uspto-grants-1996_11 |