Hydrochloric Acid → HCID 23368461, compound

HRID 1901634Notes

Reaction equation

HRID 1901634 reaction equation
C(OCC)(=O)C.[NH2:7][CH:8]([CH2:20][CH2:21][CH3:22])[CH2:9][O:10][C:11]1[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[O:13][N:12]=1.[ClH:23]>O1CCOCC1>[ClH:23].[NH2:7][CH:8]([CH2:20][CH2:21][CH3:22])[CH2:9][O:10][C:11]1[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[O:13][N:12]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 8857Ethyl AcetateHCID 23368395HCID 23368395, compound

Product 1

HCID 23368461HCID 23368461, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

To 20 ml of an ethyl acetate solution of 2 g of 3-(2-aminopentyloxy)-1,2-benzoisoxazole is added 20 ml of a dioxane solution (2.2N) of hydrogen chloride, and the crystals precipitated are collected by filtration to obtain 1.05 g of colorless, crystalline 3-(2-aminopentyloxy)-1,2-benzoisoxazole hydrochloride having a melting point of 205.8°-206.5° C.

Workup

  1. customthe crystals precipitated
  2. filtrationare collected by filtration

Sources & evidence

ORD record
ord-5c8676b4d9ff43c99c2e7ab3460facf2
Source dataset
uspto-grants-1996_11
Patent number
US05578627

Reaction notes

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