HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67733446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | HCID 67733447 | HCID 67733447 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67733446 | HCID 67733446 | — |
Reaction Steps
To a solution of 0.14 g of (R)-3-(2-amino-3-methanesulfinylpropoxy)-5-chloro-1,2-benzoisoxazole in 2 ml of methylene chloride is added 0.4 ml of a 2-propanol solution (6.5M) of hydrogen chloride, and the crystals precipitated are collected by filtration, to obtain 0.07 g of colorless, crystalline (R)-3-(2-amino-3-methanesulfinylpropoxy)-5-chloro-1,2-benzoisoxazole hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578627 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-9c07d1433e874a5b950dec9fe373fb7f |
| Source note | uspto-grants-1996_11 |