化工社化工社 化学情報印刷レポート · 研究参考用
1-Azido-3-phenylpropan-2-ol → 1-Amino-3-phenylpropan-2-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Azido-3-phenylpropan-2-ol | HCID 13764832 | — |
| 反応物 | Aluminium lithium hydride | HCID 21226445 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 1-Amino-3-phenylpropan-2-ol | HCID 3758046 | 102.7% |
反応手順
A procedure similar to that described in Preparation 13 was repeated, except that 6.0 g of 3-phenyl-2-hydroxypropylazide (prepared as described in Preparation 16), 2.6 g of lithium aluminum hydride and 300 ml of anhydrous tetrahydrofuran were used, to give 5.26 g of the title compound, melting at 64° C. to 66° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05578620 |
| 出典データセット | uspto-grants-1996_11 |
| ORD ID | ord-6c6509b68988429fab355a67dd68e532 |
| 出典メモ | uspto-grants-1996_11 |