Aluminium lithium hydride → HCID 21474756, compound

Participants

Reaction Steps

A procedure similar to that described in Preparation 13 was repeated, except that 4.30 g of 3-(4-phenylbutoxy)-2-hydroxypropylazide (prepared as described in Preparation 59), 1.31 g of lithium aluminum hydride and 120 ml of anhydrous tetrahydrofuran were used, to give 3.70 g of the title compound as a colorless oil having an Rf value of 0.08 (on silica gel thin layer chromatography, using a 10:1 by volume mixture of ethyl acetate and methanol as the developing solvent).

Provenance & Evidence