HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovaleryl chloride → HCID 9840009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovaleryl chloride | HCID 66054 | — |
| Reactant | 3-Butyn-1-ol, 4-(5-(2-thienyl)-2-thienyl)- | HCID 440357 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 9840009 | HCID 9840009 | — |
Reaction Steps
5-(4-Hydroxy-1-butynyl)-2,2'-bithiophene (1 g) was dissolved in pyridine (10 ml). Isovaleroyl chloride (1 ml) was added at room temperature, stirred for few minutes and kept overnight. The reaction mixture was treated as in example 21. Light yellowish oily product (1.06 g) was then obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578636 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-659f06058caa4604a7250c9d7caa6db9 |
| Source note | uspto-grants-1996_11 |