HuagongsheHuagongshe Chemistry Print Report · For research reference only
Palmitoyl chloride → HCID 18920431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Palmitoyl chloride | HCID 8206 | — |
| Reactant | 3-Butyn-1-ol, 4-(5-(2-thienyl)-2-thienyl)- | HCID 440357 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18920431 | HCID 18920431 | — |
Reaction Steps
5-(4-Hydroxy-1-butynyl)-2,2'-bithiophene (0.6 g) was dissolved in pyridine (10 ml). Palmitoyl chloride (1 ml) was added at room temperature, stirred for few minutes and kept overnight. The reaction mixture was treated as in example 21, and 1.2 g of light yellowish crystals were then obtained and the melting point thereof was 68°-69° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578636 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-24ab461d96914bfc861bb6ae812fd90b |
| Source note | uspto-grants-1996_11 |