HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → Methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 15837964 | HCID 15837964 | — |
| Reactant | HCID 54443108 | HCID 54443108 | — |
| Product | Methanol | HCID 887 | 17% |
| Product | HCID 15837964 | HCID 15837964 | — |
Reaction Steps
5-Methoxy-2-methyl-1-[(3-pyridyl)methyl]-1H-indole-3-acetic acid hydrazide. Using the method described in Example 1, Part G, 340 mg (1.0 mmol) of 5-methoxy-2-methyl-1-[(3-pyridyl)methyl]-1H-indole-3-acetic acid ethyl ester was reacted with 1.0 mL of hydrazine to give on crystallization from MeOH 54 mg (17% yield) of 5-methoxy-2-methyl-1-[(3-pyridyl)methyl]-1H-indole-3-acetic acid hydrazide, mp 153°-154.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578634 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-d7d577eed6624607beb7a189ebfb319b |
| Source note | uspto-grants-1996_11 |