HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diboron → HCID 13103378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diboron | HCID 6328200 | — |
| Reactant | 12-formyl-2-methyl-3,4-dioxo-1,3,4,14b-tetrahydro-10H-pyrazino[1,2-a]pyrrolo[2,1-c][1,4]benzodiazepine | HCID 12837784 | — |
| Product | HCID 13103378 | HCID 13103378 | — |
Reaction Steps
According to the method illustrated by Examples 1 and 2, the 12-formyl-2-methyl-3,4-dioxo-1,3,4,14b-tetrahydro-10H-pyrazino[1,2-a]pyrrolo[2,1-c][1,4]benzodiazepine is reduced with diborane, to yield the 2,12-dimethyl-1,3,4,14b-tetrahydro-10H-pyrazino[1,2-a]pyrrolo[2,1-c][1,4]benzodiazepine, which is converted into its monomaleate melting at 173°-175°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362666 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-59b3b9f0f84544b59e6b6fef7989814c |
| Source note | uspto-grants-1982_12 |