HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-AMino-1H-pyrazol-1-yl)propanenitrile → HCID 54298987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-AMino-1H-pyrazol-1-yl)propanenitrile | HCID 12245933 | — |
| Reactant | 1,1,1-Trifluoro-2-isothiocyanatoethane | HCID 13883777 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54298987 | HCID 54298987 | — |
Reaction Steps
2,2,2-Trifluoroethylisothiocyanate (3.4 g.) was added to a solution of 3-amino-1-(2-cyanoethyl)-pyrazole (2.72 g.) in acetonitrile (10 ml.) and the solution left at room temperature for 18 hours. The mixture was evaporated to dryness and the residue recrystallised from ethanol to give 3-[3-(2,2,2-trifluoroethyl)thioureido]-1-(2-cyanoethyl)pyrazole, m.p. 164°-165°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362728 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-64eb143b8f6f40d9b506d8cf040ea338 |
| Source note | uspto-grants-1982_12 |