HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Myristoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 131712894 | HCID 131712894 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Myristoyl chloride | HCID 66986 | 100% |
Reaction Steps
4.5 g of intermediate B obtained by the example (b) was dissolved in 50 ml of benzene and stirred at the room temperature, and 7 ml of thionylchloride was then added therein. After stirred to make reflus for three hours, concentration was made, and 4.7 g (100%) of brown oil have been obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362810 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-6707d3ecf0c74586ae67c8496270ee9e |
| Source note | uspto-grants-1982_12 |